1. Home
  2. 研究室紹介
  3. バトンゾーン研究推進プログラム
  4. 理研-JEOL連携センター

バトンゾーン研究推進プログラム ナノ結晶解析連携ユニット

ユニットリーダー 西山 裕介(Ph.D.)


西山 裕介 (Ph.D.)

わたしたちの研究ユニットでは、ナノメーターからマイクロメーターのサイズの非常に小さな微結晶から、結晶構造を解く新規手法の開発と応用に注力しています。電子回折と固体NMRを組み合わせた、electron and NMR nanocrystallographyにより、水素原子の位置まで精密に構造を決定することができます。応用範囲は、さまざまな分野にまたがっており、医薬品、タンパク質、生体物質、有機無機ハイブリッド材料などの構造解析を進めています。


  • 化学


  • 総合理工


  • 固体NMR
  • 電子回折
  • ナノ結晶学


  • 1. Nghia Tuan Duong*, Yusuke Nishiyama*.
    "Detection of remote proton-nitrogen correlations by 1H-detected 14N overtone solid-state NMR at fast MAS"
    Phys. Chem. Chem. Phys. in press. DOI: 10.1039/D2CP00155A
  • 2. Nghia Tuan Duong, Vipin Agarwal, Yusuke Nishiyama*.
    "Separating an overlapped 1H peak and identifying its 1H-1H correlations with the use of single-channel 1H solid-state NMR at fast MAS"
    Solid State Nucl. Magn. Reson. 117 (2022) 101774. DOI: 10.1016/j.ssnmr.2022.101774
  • 3. Ekta Nehra, Neelam Sehrawat, Takeshi Kobayashi, Yusuke Nishiyama*, Manoj Kumar Pandey*.
    "Proton-detected 15N-1H dipolar coupling/1H chemical shift correlation experiment for the measurement of NH distances in biological solids under fast MAS solid-state NMR"
    J. Magn. Reson. Open, 10-11 (2022) 100028. DOI: 10.1016/j.jmro.2021.100028
  • 4. Ziya Liu, Kun Zhang, Guoji Huang, Bingqing Xu*, You-lee Hong, Xiaowei Wu, Yusuke Nishiyama, Satoshi Horike*, Gen Zhang* and Susumu Kitagawa.
    "High-Processable COF Gel Electrolyte Enabled by Side Chain Engineering for Lithium-ion Battery"
    Angew. Chem. Int. Ed. 61 (2022) e202110695. DOI: 10.1002/ange.202110695
  • 5. Alons Lends*, Mélanie Berbon, Birgit Habenstein, Yusuke Nishiyama*, and Antoine Loquet*.
    "Protein resonance assignment by solid-state NMR based on 1H-detected 13C double-quantum spectroscopy at fast MAS"
    J. Biomol. NMR 75 (2021) 417-427. DOI: 10.1007/s10858-021-00386-6
  • 6. Kentaro Kadota, You-lee Hong, Yusuke Nishiyama, Easan Sivaniah, Daniel Packwood, and Satoshi Horike*.
    "One-Pot, Room-Temperature Conversion of CO2 into Porous Metal–Organic Frameworks"
    J. Am. Chem. Soc. (2021) J. Am. Chem. Soc. 143 (2021) 16750-16757. DOI: 10.1021/jacs.1c08227
  • 7. Rognchun Zhang*, Vipin Agarwal*, Yusuke Nishiyama*.
    "Proton Triple-Quantum Solid-State NMR spectroscopy at slow MAS ~10 kHz"
    J. Magn. Reson. Open 8-9 (2021) 100020. DOI: 10.1016/j.jmro.2021.100020
  • 8. Zhen Shan, Miaomiao Wu, Zhangjie Gu, Yusuke Nishiyama, Gen Zhang*.
    "A Nonplanar 2D Covalent Organic Framework Derived from a Z-shaped Building Unit,"
    Chem. Comm. 57 (2021) 9236-9239. DOI: 10.1039/D1CC04103G
  • 9. Nghia Tuan Duong, Yoshitaka Aoyama, Katsumi Kawamoto, Toshio Yamazaki, Yusuke Nishiyama*.
    "Structure Solution of Nano-Crystalline Small Molecules Using MicroED and Solid-State NMR Dipolar-Based Experiments"
    Molecules 26 (2021) 4652. DOI: 10.3390/molecules26154652
  • 10. Xiaowei Wu, Ziya Liu, Hu Guo, You-lee Hong, Bingqing Xu*, Kun Zhang, Yusuke Nishiyama, Wei Jiang, Satoshi Horike, Susumu Kitagawa, Gen Zhang*.
    "Host–Guest Assembly of H-Bonding Networks in Covalent Organic Frameworks for Ultrafast and Anhydrous Proton Transfer"
    ACS Appl. Mater. Interfaces, 13 (2021) 37172-37178. DOI: 10.1021/acsami.1c09157




西山 裕介


〒230-0045 神奈川県横浜市鶴見区末広町1-7-22 理研-JEOL連携センター W123
Email: yusuke.nishiyama [at] riken.jp